This invention relates to a method of preparing a compound of formula (I):
##STR1##
The method includes reacting one or more compounds of formula (II):
##STR2##
in the presence of a base and a halogenating agent. In formulas (I) and (II) above,
each A, independently, is aryl or heteroaryl; each n, independently, is 0-3; and
each R1, independently, is C1-C10 alkyl, C3-C20
cycloalkyl, C3-C20 heterocycloalkyl, aryl, heteroaryl,
halo, cyano, nitro, ORa, NRaRb, SiRaRbRc,
COORa, OC(O)Ra, C(O)NRaRb, N(Ra)—C(O)Rb,
or SO3Ra; wherein each of Ra, Rb, and
Rc, independently, is H, C1-C10 alkyl, C3-C20
cycloalkyl, C3-C20 heterocycloalkyl, aryl, or heteroaryl;
thereby producing the compound of formula (I) in a one-pot reaction. This invention
also relates to the compounds prepared by the method described above.