A process for the regeneration of a deactivated zeolite beta catalyst such
as rare earth promoted zeolite beta catalyst deactivated in the course of
an aromatic alkylation reaction. A zeolite beta conversion catalyst
deactivated with the deposition of coke is heated to a temperature in
excess of 300.degree. C. in an oxygen-free environment. An oxidative
regeneration gas is supplied to the catalyst bed with oxidation of a
portion of a relatively porous coke component to produce an exotherm
moving through the catalyst bed. At least one of the temperature and
oxygen content of the gas is progressively increased to oxidize a porous
component of the coke. Regeneration gas is supplied having at least one
of an increased oxygen content or increased temperature to oxidize a less
porous refractory component of the coke. The regeneration process is
completed by passing an inert gas through the catalyst bed at a reduced
temperature.