A process and apparatus for catalytic production of single walled carbon
nanotubes. Catalytic particles are exposed to different process
conditions at successive stages wherein the catalytic particles do not
come in contact with reactive (catalytic) gases until preferred process
conditions have been attained, thereby controlling the quantity and form
of carbon nanotubes produced. The reaction gas is preferably provided at
a high space velocity to minimize CO.sub.2 build-up. The process also
contemplates processes and apparatus which recycle and reuse the gases
and catalytic particulate materials, thereby maximizing cost efficiency,
reducing wastes, reducing the need for additional raw materials, and
producing the carbon nanotubes, especially SWNTs, in greater quantities
and for lower costs.