A hydrometallurgical process based on pressure leaching at elevated
temperature for recovering nickel from nickel oxide ores, characterized
by a simplified and efficient process as a whole, realizing a simplified
leaching stage, reduced neutralizer consumption and precipitate
production in the neutralization stage, and efficient use of recycled
water.The hydrometallurgical process of the present invention, comprising
a leaching stage which stirs the slurried ore in the presence of sulfuric
acid at 220 to 280.degree. C. to produce the leached slurry; solid-liquid
separation stage which washes the leached slurry in multi-stages to
produce the pregnant liquor and leached residue, the former containing
nickel and cobalt; neutralization stage which treats the pregnant liquor
in the presence of calcium carbonate incorporated to keep the pH level at
4 or less, while suppressing oxidation of the liquor, to produce the
neutralization precipitate slurry and mother liquor for nickel recovery,
the former containing trivalent iron; and a sulfide precipitation stage
which blows hydrogen sulfide gas into the mother liquor to produce the
sulfide solution and barren liquor, the former containing nickel and
cobalt.