A structural body comprising a substrate and a structural layer formed on
the substrate through an air gap in which the structural layer functions
as a micro movable element is produced by a process comprising a
film-deposition step of successively forming a sacrificial layer made of
a silicon oxide film and the structural layer on the substrate, an air
gap-forming step of removing the sacrificial layer by etching with a
treating fluid to form the air gap between the substrate and the
structural layer, and a cleaning step. By using a supercritical carbon
dioxide fluid containing a fluorine compound, a water-soluble organic
solvent and water as the treating fluid, the sacrificial layer is removed
in a short period of time with a small amount of the treating fluid
without any damage to the structural body.