The invention concerns a process for making a fibrillated polypyridobisimidazole floc comprising the steps of: cutting polypyridobisimidazole filaments to an average cut length of from about 0.5 to 10 mm; and applying energy to the polypyridobisimidazole filaments to produce a fibrillated floc having essentially the same average cut length after the application of energy as before the application of energy; where the fibrillated floc having a Canadian Standard Freeness (CSF), when dispersed in water by itself, of from about 400 to 750 ml.