A method is shown for raising the pH of a cyanide leach solution of the type used in a heap leaching mining operation. Lime slurry is mixed with a side stream of barren cyanide solution in a reactor vessel in order to remove carbonate hardness, to regenerate the hydroxide alkalinity and to raise the pH of the resulting recausticized leach solution. A portion of the calcium carbonate precipitate formed in the reactor vessel is retained in order to encourage further crystal growth. Overflow from the reactor vessel passes through one or more cyclone separation stages in order to remove particulate solids. A cyclone overflow stream is directed back to the process to upwardly adjust the pH of the bulk of the barren cyanide solution. A cyclone underflow stream is directed back to the reactor vessel to provide seed crystal nuclei for precipitate growth. Periodically, precipitate grains are drained from the bottom of the reactor vessel, water-washed to recover cyanide solution, and discharged as carbonate sand and lime grit.

 
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