A process for purifying monoterpenes, including the steps of: providing a
monoterpene comprising alpha terpinene of about 90% or greater purity and
comprising an oxygen-containing impurity compound selected from the group
consisting of 1,8-cineole, 1,4,-cineole, and mixtures thereof; providing
an activated silica gel preparative chromatographic column; contacting
the monoterpene with the column, wherein the oxygen-containing impurity
compounds are retained on the column; recovering monterpenes depleted of
oxygen-containing impurity compounds from the column by applying a
pressure above atmospheric from a gas source without the use of a
solvent; and removing the oxygen-containing impurity compounds by
contacting the column with an alcohol.