The present invention relates a method for preparing nanometer
electrocatalyst for proton exchange membrane fuel cells, comprising the
steps of: 1) adding in water a platinum halogen compound or a mixture of a
platinum halogen compound and a ruthenium halogen compound, and active
carbon, the amount of noble metal in the solution is 0.5-10 g/L, and the
amount of active carbon is 0.05-2 g/L; 2) adjusting the pH of the solution
to 2.5-10.5 with potassium hydroxide and/or ammonium hydroxide; 3) adding
dropwise a reducing agent to an amount of 2.5 to 5 times in excess of that
of the noble metal in moles, and allowing the reduction reaction to
proceed; 4) filtering off the liquid and washing the remains; and 6)
drying the remains. The catalysts prepared by the present invention have
uniform particle sizes in the range of 4.+-.0.5 nm, and superior
electrochemical properties.