This invention relates generally to a single-wall carbon nanotube (SWNT) purification
process and more particularly to a purification process that comprises heating
the SWNT-containing felt under oxidizing conditions to remove the amorphous carbon
deposits and other contaminating materials. In a preferred mode of this purification
procedure, the felt is heated in an aqueous solution of an inorganic oxidant, such
as nitric acid, a mixture of hydrogen peroxide and sulfuric acid, or a potassium
permanganate. Preferably, SWNT-containing felts are refluxed in an aqueous solution
of an oxidizing acid at a concentration high enough to etch away amorphous carbon
deposits within a practical time frame, but not so high that the single-wall carbon
nanotube material will be etched to a significant degree. When material having
a high proportion of SWNT is purified, the preparation produced will be enriched
in single-wall nanotubes, so that the SWNT are substantially free of other material.