A process/apparatus is disclosed for continuously separating a liquid medium
comprising
diluent and unreacted monomers from a polymerization effluent comprising diluent,
unreacted monomers and polymer solids, comprising a continuous discharge of the
polymerization effluent from a slurry reactor through a discharge valve and transfer
conduit into a first intermediate pressure flash tank with a conical bottom defined
by substantially straight sides inclined at an angle to that of horizontal equal
to or greater than the angle of slide of the slurry/polymer solids and an exit
seal chamber of such diameter (d) and length (l) as to maintain a desired volume
of concentrated polymer solids/slurry in the exit seal chamber such as to form
a pressure seal while continuously discharging a plug flow of concentrated polymer
solids/slurry bottom product of said first flash tank from the exit seal chamber
through a seal chamber exit reducer with inclined sides defined by substantially
straight sides inclined at an angle to that of horizontal equal to or greater than
the angle of slide of the polymer solids which remain after removal of about 50
to 100% of the inert diluent therefrom to a second flash tank at a lower pressure.