The present invention relates to a method for manufacturing a transition
metal boride powder. The method for manufacturing a transition metal
boride powder includes: i) manufacturing a mixed powder by mixing a
transition metal halogenide powder and an alkali metal borohydride
powder; ii) charging the mixed powder and a plurality of balls into a
reaction vessel; iii) charging an inert gas into the reaction vessel and
sealing the reaction vessel; iv) high energy ball milling the mixed
powder and manufacturing a composite powder containing a transition metal
boride and an alkali metal halogenide; v) washing the composite powder in
water, dissolving the alkali metal halogenide in the water and filtering
the transition metal borides; and vi) drying the filtered transition
metal boride and collecting the transition metal boride powder.