Process of manufacturing carbon-carbon composite preform by: (i.)
arranging batch of carbon fiber preforms in infiltration vessel; (ii.)
flooding vessel with hot liquid phase pitch at atmospheric pressure in
inert atmosphere; (iii.) raising pressure in infiltration vessel to
elevated pressure, and then slowly lowering pressure; and (iv.) repeating
step (iii.). An apparatus that may be used is a heated infiltration
vessel capable of operating at pressures above 100 psi, possible equipped
with means to circulate heated pitch inside the vessel, in order to
facilitate heat transfer into the carbon fiber preforms being infiltrated
by the pitch. The need for a vacuum pump is eliminated, and the time
spent heating the preform is substantially reduced. Instead of vacuum,
cycled high pressure is employed to infiltrate carbon fiber preforms with
pitch. The use of preheated pitch as a heat transfer agent avoids the
slow transfer of heat into the preform prior to infiltration.