A method for fabricating dielectric barrier layers in integrated circuit structures
such as damascene structures is provided. In one embodiment, a low-k dielectric
layer formed on a substrate is provided. The low-k dielectric layer has at least
one opening exposing an underlying metal layer. A first silicon carbide barrier
layer is formed to conformally cover the exposed surfaces of the opening. A portion
of the first silicon carbide barrier layer above the low-k dielectric layer and
over the bottom of the opening is converted with an oxidation treatment into a
layer of silicon oxide. The silicon oxide layer is removed above the low-k dielectric
layer and from the bottom of the opening. The opening is filled with a conductive
layer in electrical contact with the underlying metal layer. The conductive layer
is removed above the low-k dielectric layer to a predetermined depth below the
low-k dielectric layer to define a recess therebelow. A second silicon carbide
barrier layer is formed to cover the recess and above the low-k dielectric layer
and the first silicon carbide barrier layer so as to seal the top of the structure.
A portion of the second silicon carbide barrier layer above the low-k dielectric
layer is converted with an oxidation treatment into a layer of silicon oxide. The
layer of silicon oxide is then removed and the metal conductive layer is fully
encapsulated by the silicon carbide barrier layer.